2WFD
Structure of the human cytosolic leucyl-tRNA synthetase editing domain
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 65 |
格子定数 [Å] | 94.540, 94.540, 148.820 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 29.240 - 3.250 |
R因子 | 0.204 |
Rwork | 0.202 |
R-free | 0.24000 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.318 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELXD (SHARP) |
Refinement software | REFMAC (5.5.0070) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 30.000 | 3.300 |
分解能 [Å] (高) | 3.000 | 3.250 |
Rmerge_l_obs | 0.150 | 0.660 |
独立反射数 | 15008 | |
<I/σ(I)> | 7.46 | 1.98 |
完全性 [%] | 99.8 | 99.5 |
冗長性 | 3.12 | 3.16 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 0.2 M SODIUM CITRATE TRIBASIC DIHYDRATE PH 8.3, 20% W/V POLYETHYLENE GLYCOL 3350 |