2V12
Crystal Structure of Renin with Inhibitor 8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR571 |
Temperature [K] | 10 |
Detector technology | AREA DETECTOR |
Collection date | 1993-01-01 |
Detector | DELFT |
Spacegroup name | P 21 3 |
Unit cell lengths | 142.900, 142.900, 142.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 3.200 |
R-factor | 0.236 |
Rwork | 0.236 |
Structure solution method | OTHER |
RMSD bond length | 0.018 |
RMSD bond angle | 3.570 |
Data reduction software | MADNESS |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 3.200 |
Rmerge | 0.130 |
Number of reflections | 15411 |
Completeness [%] | 92.0 |
Redundancy | 2.81 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | pH 4.50 |