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2R88

Crystal structure of the long-chain fatty acid transporter FadL mutant delta S3 kink

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X6A
Synchrotron siteNSLS
BeamlineX6A
Temperature [K]100
Detector technologyCCD
Collection date2007-04-22
DetectorADSC QUANTUM 210
Wavelength(s)1.1
Spacegroup nameC 2 2 21
Unit cell lengths91.327, 91.370, 267.317
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution10.000 - 2.600
R-factor0.262
Rwork0.262
R-free0.29400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1t16
RMSD bond length0.008
RMSD bond angle1.400
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]31.9002.640
High resolution limit [Å]2.5502.550
Rmerge0.0790.563
Number of reflections33965
<I/σ(I)>13.92.4
Completeness [%]91.984.2
Redundancy8.94.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.529530% PEG 5000 MME, 0.2M ammonium sulfate, 0.1M MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K

217705

건을2024-03-27부터공개중

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