2QG0
HSP90 complexed with A943037
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-BM |
Synchrotron site | APS |
Beamline | 17-BM |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2006-03-24 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 113.346, 89.144, 64.456 |
格子定数 [度] | 90.00, 121.45, 90.00 |
精密化法
残基 | 19.860 - 1.850 |
R因子 | 0.241 |
Rwork | 0.229 |
R-free | 0.28500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1yer |
結合長の平均二乗偏差(RMSD) [Å] | 0.005 |
結合角の平均二乗偏差(RMSD) [度] | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNX (2002) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 20.000 | 1.920 |
分解能 [Å] (高) | 1.850 | 1.850 |
独立反射数 | 45919 | |
<I/σ(I)> | 27.7 | 12.8 |
完全性 [%] | 98.5 | 93.7 |
冗長性 | 3.2 | 3.1 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 40 mg/ml protein with a reservoir solution of 20-28 %(w/v)PEG 3350, 0.1 M Bis-Tris-Propane PH 6.5, 0.2 M Sodium chloride, VAPOR DIFFUSION, HANGING DROP, temperature 277K |