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2Q3F

X-ray crystal structure of putative human Ras-related GTP binding D in complex with GMPPNP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 17-ID
Synchrotron siteAPS
Beamline17-ID
Temperature [K]100
Detector technologyCCD
Collection date2007-04-14
DetectorADSC QUANTUM 210
Wavelength(s)0.97942, 1.0
Spacegroup nameP 1 21 1
Unit cell lengths47.730, 67.130, 66.360
Unit cell angles90.00, 110.92, 90.00
Refinement procedure
Resolution50.000 - 2.100
R-factor0.223
Rwork0.221
R-free0.26800
Structure solution methodSAD
RMSD bond length0.006
RMSD bond angle1.280
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSOLVE
Refinement softwareCNS (1.2)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.120
High resolution limit [Å]2.0502.050
Rmerge0.542
Number of reflections24803
<I/σ(I)>2.4
Completeness [%]99.899.1
Redundancy4.13.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION8.429831% PEG4000, 0.2M sodium acetate and 0.1M Tris HCl, pH 8.4, VAPOR DIFFUSION, temperature 298K

217705

数据于2024-03-27公开中

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