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2PGI

THE CRYSTAL STRUCTURE OF PHOSPHOGLUCOSE ISOMERASE-AN ENZYME WITH AUTOCRINE MOTILITY FACTOR ACTIVITY IN TUMOR CELLS

Experimental procedure
Source typeROTATING ANODE
Source detailsRIGAKU RUH3R
Temperature [K]287
Detector technologyIMAGE PLATE
Collection date1997-07-25
DetectorRIGAKU RAXIS II
Spacegroup nameI 2 2 2
格子定数 [Å]75.100, 93.730, 171.900
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基8.000 - 2.300
R因子0.185
Rwork0.185
R-free0.25800

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Structure solution methodMIRAS
結合長の平均二乗偏差(RMSD) [Å]0.012
結合角の平均二乗偏差(RMSD) [度]26.100

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Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareX-PLOR (3.1)
Refinement softwareX-PLOR (3.1)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)30.7002.380
分解能 [Å] (高)2.3002.300
Rmerge_l_obs0.0700.362

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Total number of observations104060

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独立反射数24024
<I/σ(I)>123.2
完全性 [%]93.983.4
冗長性4.33.1
結晶化条件
結晶ID方法pH温度溶液条件
1Vapor diffusion, hanging drop

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7pH 7.0
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11dropprotein (mg/ml)
21drop6-phosphogluconate (mM)
31dropphosphate (mM)
41reservoirphosphate (mM)
51reservoirammonium phosphate (M)

217705

件を2024-03-27に公開中

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