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2OKK

The X-ray crystal structure of the 65kDa isoform of Glutamic Acid Decarboxylase (GAD65)

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 17-ID
Synchrotron siteAPS
Beamline17-ID
Temperature [K]100
Detector technologyCCD
Collection date2006-04-01
DetectorADSC QUANTUM 4
Wavelength(s)1.000
Spacegroup nameC 2 2 21
格子定数 [Å]78.251, 99.057, 120.009
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基37.190 - 2.300
R因子0.2
Rwork0.196
R-free0.25600
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2okj
結合長の平均二乗偏差(RMSD) [Å]0.009
結合角の平均二乗偏差(RMSD) [度]1.352
Data reduction softwareHKL-2000
Data scaling softwareSCALA (CCP4_3.2.17 23/9/2005)
Phasing softwarePHASER
Refinement softwareREFMAC (5.2.0019)
Quality characteristics
 OverallInner shellOuter shell
分解能 [Å] (低)37.19054.6402.420
分解能 [Å] (高)2.3007.2702.300
Total number of observations224711442
独立反射数20717
完全性 [%]91.8698.85
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, HANGING DROP6.229320% ethanol, 100 mM MES, 10 mM 2-mercaptoethanol, 20 mM CaCl2, pH 6.2, VAPOR DIFFUSION, HANGING DROP, temperature 293K

217705

件を2024-03-27に公開中

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