Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-07-12 |
Detector | RIGAKU |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 49.187, 63.765, 64.742 |
格子定数 [度] | 90.00, 91.81, 90.00 |
精密化法
残基 | 45.410 - 1.800 |
R因子 | 0.189 |
Rwork | 0.186 |
R-free | 0.23700 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.012 |
結合角の平均二乗偏差(RMSD) [度] | 1.476 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 45.410 | 1.860 |
分解能 [Å] (高) | 1.800 | 1.800 |
独立反射数 | 33633 | |
完全性 [%] | 89.7 | 49.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 300 | 0.1M BICINE pH 9.0, 27% PEG3350, 0.2M MgCl2, PH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 300K |