2O0L
Human spermidine synthase
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-04-13 |
Detector | RIGAKU |
Wavelength(s) | 1.54178 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 58.323, 60.593, 86.667 |
格子定数 [度] | 90.00, 108.96, 90.00 |
精密化法
残基 | 81.920 - 1.990 |
R因子 | 0.20923 |
Rwork | 0.206 |
R-free | 0.26755 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.017 |
結合角の平均二乗偏差(RMSD) [度] | 1.521 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 81.920 |
分解能 [Å] (高) | 1.990 |
Rmerge_l_obs | 0.121 |
独立反射数 | 36969 |
<I/σ(I)> | 7.5 |
完全性 [%] | 99.4 |
冗長性 | 5.3 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 300 | 20% PEG 3350, 0.2M Mg(OAc)2, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 300K |