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2NGR

TRANSITION STATE COMPLEX FOR GTP HYDROLYSIS BY CDC42: COMPARISONS OF THE HIGH RESOLUTION STRUCTURES FOR CDC42 BOUND TO THE ACTIVE AND CATALYTICALLY COMPROMISED FORMS OF THE CDC42-GAP.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE F1
Synchrotron siteCHESS
BeamlineF1
Temperature [K]120
Detector technologyCCD
Collection date1998-03-01
DetectorADSC
Spacegroup nameP 21 21 21
Unit cell lengths52.820, 67.690, 131.060
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution22.000 - 1.900
R-factor0.253
Rwork0.253
R-free0.29300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1grn
RMSD bond length0.006
RMSD bond angle23.010

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Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareX-PLOR
Refinement softwareX-PLOR (3.851)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.000
High resolution limit [Å]1.9001.900
Rmerge0.098

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Total number of observations394559

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Number of reflections40680

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<I/σ(I)>13.43.5
Completeness [%]99.499.6
Redundancy9.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

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6pH 6.0
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirPEG400015-20 (%(w/v))
21reservoirmagnesium acetate0.2 (M)
31reservoir0.10 (mM)
41reservoir10-30 (mM)

217705

건을2024-03-27부터공개중

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