Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 1997-12-09 |
Detector | MARRESEARCH |
Spacegroup name | H 3 2 |
格子定数 [Å] | 288.000, 288.000, 653.000 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 40.000 - 2.850 |
R因子 | 0.2 |
Rwork | 0.200 |
R-free | 0.22000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | MS2 RECOMBINANT CAPSIDS |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.0) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 40.000 | 2.950 |
分解能 [Å] (高) | 2.850 | 2.850 |
Rmerge_l_obs | 0.130 | 0.360 |
独立反射数 | 161000 | |
完全性 [%] | 67.0 | 34 |
冗長性 | 2.7 | 1.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 7.4 | pH 7.40 |