Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 1997-12-09 |
Detector | MARRESEARCH |
Spacegroup name | H 3 2 |
Unit cell lengths | 288.000, 288.000, 653.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 2.850 |
R-factor | 0.2 |
Rwork | 0.200 |
R-free | 0.22000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | MS2 RECOMBINANT CAPSIDS |
RMSD bond length | 0.007 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.950 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.130 | 0.360 |
Number of reflections | 161000 | |
Completeness [%] | 67.0 | 34 |
Redundancy | 2.7 | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | pH 7.40 |