2IX2
Crystal structure of the heterotrimeric PCNA from Sulfolobus solfataricus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX14.1 |
Synchrotron site | SRS |
Beamline | PX14.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.808, 78.798, 125.611 |
Unit cell angles | 90.00, 100.51, 90.00 |
Refinement procedure
Resolution | 48.620 - 2.200 |
R-factor | 0.22 |
Rwork | 0.217 |
R-free | 0.27300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ud9 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.355 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.060 | 0.380 |
Number of reflections | 43983 | |
<I/σ(I)> | 13.4 | 1.9 |
Completeness [%] | 91.0 | 93 |
Redundancy | 2.3 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |