2IPX
Human Fibrillarin
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-10-05 |
Detector | RIGAKU |
Wavelength(s) | 1.54 |
Spacegroup name | P 41 21 2 |
格子定数 [Å] | 57.261, 57.261, 135.028 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 39.000 - 1.820 |
R因子 | 0.20241 |
Rwork | 0.200 |
R-free | 0.24552 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1fbn |
結合長の平均二乗偏差(RMSD) [Å] | 0.012 |
結合角の平均二乗偏差(RMSD) [度] | 1.402 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | REFMAC (5.2.0019) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 39.000 | 1.860 |
分解能 [Å] (高) | 1.800 | 1.800 |
Rmerge_l_obs | 0.095 | 0.574 |
独立反射数 | 20921 | |
<I/σ(I)> | 11.3 | 1.6 |
完全性 [%] | 96.3 | 65.4 |
冗長性 | 11.9 | 4.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 300 | 20% PEG3350, 0.2 M CaCl2, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 300K |