2HTW

N4 neuraminidase in complex with DANA

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2005-05-05
Detector	RIGAKU RAXIS IIC
Wavelength(s)	1.54
Spacegroup name	I 4 3 2
格子定数 [Å]	193.400, 193.400, 193.400
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	30.000 - 3.500
R因子	0.217
Rwork	0.217
R-free	0.29500
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	CNS (1.1)

Quality characteristics

	Overall
分解能 [Å] (低)	30.000
分解能 [Å] (高)	3.500
独立反射数	7998
完全性 [%]	99.2

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	7.5	293	HEPES, PEG3350, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K