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2HBH

Crystal structure of Vitamin D nuclear receptor ligand binding domain bound to a locked side-chain analog of calcitriol and SRC-1 peptide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-3
Synchrotron siteESRF
BeamlineID14-3
Temperature [K]100
Detector technologyCCD
Collection date2003-10-12
DetectorMAR CCD 165 mm
Wavelength(s)0.931
Spacegroup nameP 65 2 2
Unit cell lengths65.682, 65.682, 265.096
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution20.000 - 2.650
R-factor0.206
Rwork0.203
R-free0.26100
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2hc4
RMSD bond length0.006
RMSD bond angle1.120
Data scaling softwareHKL-2000
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.740
High resolution limit [Å]2.6002.650
Number of reflections10531
Completeness [%]98.698.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.5298Li sulfate 1.6M, Mg sulfate 50mM, Bis Tris 0.1M, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K

217705

数据于2024-03-27公开中

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