2HA8
Methyltransferase Domain of Human TAR (HIV-1) RNA binding protein 1
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-03 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 41.237, 86.930, 48.266 |
格子定数 [度] | 90.00, 100.85, 90.00 |
精密化法
残基 | 47.400 - 1.600 |
R因子 | 0.17839 |
Rwork | 0.177 |
R-free | 0.20882 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.011 |
結合角の平均二乗偏差(RMSD) [度] | 1.385 |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 47.400 | 1.640 |
分解能 [Å] (高) | 1.600 | 1.600 |
独立反射数 | 42523 | |
完全性 [%] | 96.6 | 67.7 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 300 | 20% PEG 5kMME, 0.1 M Bis-Tris, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 300K |