2GKW

Key contacts promote recongnito of BAFF-R by TRAF3

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU300
Detector technology	IMAGE PLATE
Collection date	2003-10-20
Detector	RIGAKU RAXIS IV
Wavelength(s)	1.5418
Spacegroup name	P 3 2 1
格子定数 [Å]	83.500, 83.500, 78.000
格子定数 [度]	90.00, 90.00, 120.00

精密化法

残基	14.850 - 2.700
R因子	0.22
Rwork	0.220
R-free	0.26000
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1fll
結合長の平均二乗偏差(RMSD) [Å]	0.008
結合角の平均二乗偏差(RMSD) [度]	1.300
Data reduction software	CrystalClear ((MSC/RIGAKU))
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS (1.0)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	15.000	2.800
分解能 [Å] (高)	2.700	2.700
独立反射数	8860
完全性 [%]	99.3	80.3

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	6.5	298	15% PEG 4000, 0.1 M MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K