Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-6 |
Temperature [K] | 292 |
Detector technology | FILM |
Collection date | 1981-01-01 |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 317.270, 304.030, 184.600 |
格子定数 [度] | 90.00, 94.36, 90.00 |
精密化法
残基 | 7.500 - 2.450 |
Rwork | 0.273 |
Structure solution method | OTHER |
結合長の平均二乗偏差(RMSD) [Å] | 0.016 |
結合角の平均二乗偏差(RMSD) [度] | 29.700 * |
Data reduction software | FILME |
Data scaling software | PURDUE (DATA PROCESSING PACKAGE) |
Refinement software | FRODO |
Quality characteristics
Overall | |
分解能 [Å] (低) | 24.730 |
分解能 [Å] (高) | 2.450 |
Rmerge_l_obs | 0.140 |
独立反射数 | 503000 |
完全性 [%] | 76.0 |
冗長性 | 1.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | Microdialysis * | 6.5 * |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | 1 | virus | 10-12 (g/l) | |
2 | 1 | 1 | 1 (mM) | ||
3 | 1 | 1 | sodium phosphate | 50 (mM) |