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2B54

Human cyclin dependent kinase 2 (CKD2)complexed with DIN-232305

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]277
Detector technologyIMAGE PLATE
Collection date1997-10-26
DetectorRIGAKU RAXIS II
Spacegroup nameP 21 21 21
Unit cell lengths72.970, 73.160, 54.260
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution37.440 - 1.850
Rwork0.158
R-free0.26300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)IN-HOUSE CDK2 MODEL
RMSD bond length0.154
RMSD bond angle9.500
Data reduction softwareSCALE ((RIGAKU))
Data scaling softwareSCALE ((RIGAKU))
Phasing softwareX-PLOR
Refinement softwareCNX (2002)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]37.4401.870
High resolution limit [Å]1.8401.840
Rmerge0.0990.457
Number of reflections21779
<I/σ(I)>3.10.5
Completeness [%]83.767.3
Redundancy2.21.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.4291100mM HEPES pH 7.4, 50mM Ammonium Acetate, 2mM DTT, 4-14% PEG 4000, VAPOR DIFFUSION, SITTING DROP, temperature 291K

217705

数据于2024-03-27公开中

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