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2AXJ

Crystal structures of T cell receptor beta chains related to rheumatoid arthritis

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X25
Synchrotron siteNSLS
BeamlineX25
Temperature [K]100
Detector technologyCCD
Collection date2002-10-18
DetectorADSC QUANTUM 4
Wavelength(s)1.1
Spacegroup nameP 63 2 2
Unit cell lengths187.478, 187.478, 86.679
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution41.870 - 2.650
R-factor0.233
Rwork0.233
R-free0.28600
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)2axh
RMSD bond length0.008
RMSD bond angle1.300
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.740
High resolution limit [Å]2.6502.650
Rmerge0.0750.614
Number of reflections25627
<I/σ(I)>17.81.8
Completeness [%]96.177.5
Redundancy3.93.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52930.6-0.7 M sodium citrate, 0.1 M HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K

217705

数据于2024-03-27公开中

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