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2A65

Crystal structure of LEUTAA, a bacterial homolog of Na+/Cl--dependent neurotransmitter transporters

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.2
Synchrotron siteALS
Beamline8.2.2
Temperature [K]100
Detector technologyCCD
Collection date2004-12-12
DetectorADSC QUANTUM 315
Wavelength(s)0.9950
Spacegroup nameC 1 2 1
Unit cell lengths87.860, 86.310, 81.020
Unit cell angles90.00, 95.73, 90.00
Refinement procedure
Resolution50.000 - 1.650
Rwork0.199
R-free0.21700
Structure solution methodMAD
RMSD bond length0.005
RMSD bond angle1.110
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareSOLVE
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.710
High resolution limit [Å]1.6501.650
Number of reflections70306
<I/σ(I)>30.51.81
Completeness [%]97.385.9
Redundancy4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7291PEGMME550, NaCl, HEPES, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K
1VAPOR DIFFUSION, HANGING DROP7291PEGMME550, NaCl, HEPES, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K
1VAPOR DIFFUSION, HANGING DROP7291PEGMME550, NaCl, HEPES, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K

217705

数据于2024-03-27公开中

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