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1Y91

Crystal structure of human CDK2 complexed with a pyrazolo[1,5-a]pyrimidine inhibitor

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RUH3R
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2003-07-09
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.5418
Spacegroup nameP 21 21 21
Unit cell lengths53.372, 71.423, 72.004
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution25.000 - 2.150
R-factor0.2009
Rwork0.196
R-free0.29511
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1b39
RMSD bond length0.022
RMSD bond angle2.076
Data reduction softwareCrystalClear ((MSC/RIGAKU))
Data scaling softwared*TREK
Phasing softwareMOLREP
Refinement softwareREFMAC (5.1.19)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.860
High resolution limit [Å]1.8001.800
Rmerge0.0850.380
Number of reflections24371
<I/σ(I)>7.82.2
Completeness [%]92.964.2
Redundancy2.651.92
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.2293Peg 3350, Hepes, Ammonium acetate, pH 7.2, VAPOR DIFFUSION, HANGING DROP, temperature 293K

217705

건을2024-03-27부터공개중

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