1W63
AP1 clathrin adaptor core
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 32 1 2 |
格子定数 [Å] | 178.140, 178.140, 1134.994 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 40.000 - 4.000 |
R因子 | 0.2972 |
Rwork | 0.297 |
R-free | 0.30970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1GW5 |
結合長の平均二乗偏差(RMSD) [Å] | 0.014 |
結合角の平均二乗偏差(RMSD) [度] | 1.861 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 39.840 | 4.100 |
分解能 [Å] (高) | 4.010 | 4.000 |
Rmerge_l_obs | 0.120 | 0.470 |
独立反射数 | 141015 | |
<I/σ(I)> | 9.4 | 2.5 |
完全性 [%] | 81.3 | 69.7 |
冗長性 | 6.5 | 4.7 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 7 | 8-9% ETHANOL, 0.1 M NA HEPES, PH 7.5, 2 MM CYSTEINE |