1VKA
Southeast Collaboratory for Structural Genomics: Hypothetical Human Protein Q15691 N-Terminal Fragment
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Detector technology | CCD |
Collection date | 2003-02-15 |
Detector | MAR CCD 165 mm |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 31.951, 47.582, 100.690 |
格子定数 [度] | 90.00, 91.74, 90.00 |
精密化法
残基 | 100.000 - 1.600 |
Rwork | 0.200 |
R-free | 0.21370 |
Structure solution method | sulfur sas |
結合長の平均二乗偏差(RMSD) [Å] | 0.014 |
結合角の平均二乗偏差(RMSD) [度] | 1.185 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE (2.03) |
Refinement software | REFMAC (refmac_5.1.24) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 50.000 | 50.000 | 1.660 |
分解能 [Å] (高) | 1.600 | 3.450 | 1.600 |
Rmerge_l_obs | 0.040 | 0.033 | 0.107 |
独立反射数 | 37287 | ||
<I/σ(I)> | 26.2 | ||
完全性 [%] | 98.2 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | Micro-batch under oil | 6.2 | 291 | pH 6.2, Micro-batch under oil, temperature 291K |
1 | Micro-batch under oil | 6.2 | 291 | pH 6.2, Micro-batch under oil, temperature 291K |