1UZG
CRYSTAL STRUCTURE OF THE DENGUE TYPE 3 VIRUS ENVELOPE PROTEIN
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-10-15 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 52.855, 68.631, 270.180 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 20.990 - 3.500 |
R因子 | 0.286 |
Rwork | 0.284 |
R-free | 0.32400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1oan |
結合長の平均二乗偏差(RMSD) [Å] | 0.009 |
結合角の平均二乗偏差(RMSD) [度] | 1.527 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 21.000 | 3.730 |
分解能 [Å] (高) | 3.600 | 3.600 |
Rmerge_l_obs | 0.120 | 0.538 |
独立反射数 | 12090 | |
<I/σ(I)> | 12.3 | 2.6 |
完全性 [%] | 91.8 | 81.1 |
冗長性 | 5 | 4.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 8.5 | 15% PEG 8K, 0.2 M LICL2, 0.1 M TRIS/HCL, PH 8.5 |