Experimental procedure
| 実験手法 | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.54 |
| Spacegroup name | I 4 2 2 |
| 格子定数 [Å] | 60.947, 60.947, 123.689 |
| 格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
| 残基 | 20.050 - 2.400 |
| Rwork | 0.279 |
| R-free | 0.36800 |
| Structure solution method | FOURIER SYNTHESIS |
| 結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
| 結合角の平均二乗偏差(RMSD) [度] | 1.400 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS |
Quality characteristics
| Overall | Outer shell | |
| 分解能 [Å] (低) | 20.050 | 2.550 |
| 分解能 [Å] (高) | 2.400 | 2.400 |
| 完全性 [%] | 89.5 |
結晶化条件
| 結晶ID | 方法 | pH | 温度 | 溶液条件 |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 289 | 0.2M AMMONIUM ACETATE, 0.1M TRI-SODIUM CITRATE, 30% MPD, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 289K |
