1U1E
Structure of e. coli uridine phosphorylase complexed to 5(phenylseleno)acyclouridine (PSAU)
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 8-BM |
Synchrotron site | APS |
Beamline | 8-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-07-25 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9790 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 91.076, 125.690, 140.899 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 48.800 - 2.001 |
R因子 | 0.21351 |
Rwork | 0.211 |
R-free | 0.23452 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.005 |
結合角の平均二乗偏差(RMSD) [度] | 0.892 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | REFMAC (5.1.24) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.070 |
分解能 [Å] (高) | 2.000 | 2.000 |
独立反射数 | 108334 | |
完全性 [%] | 99.1 | 94.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 295 | PEG 4000, MES, GLYCEROL, PH 6.2, VAPOR DIFFUSION, HANGING DROP, temperature 295K |