1SEN

Endoplasmic reticulum protein Rp19 O95881

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-ID
Synchrotron site	APS
Beamline	22-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2003-12-19
Detector	MARRESEARCH
Wavelength(s)	1.07
Spacegroup name	P 21 21 21
格子定数 [Å]	48.986, 50.556, 59.386
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	38.633 - 1.199
Rwork	0.162
R-free	0.18350
Structure solution method	MIR
結合長の平均二乗偏差(RMSD) [Å]	0.011
結合角の平均二乗偏差(RMSD) [度]	5.538
Data scaling software	SCALEPACK
Phasing software	SOLVE (2.03)
Refinement software	REFMAC (refmac_5.1.24)

Quality characteristics

	Overall
分解能 [Å] (低)	38.633
分解能 [Å] (高)	1.199
独立反射数	42206

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	modified batch crystallization	7	291	12% PEG 4000, 100mM Na Hepes, 100mM NaCl, pH 7.0, modified batch crystallization, temperature 291K