1RUY
1930 Swine H1 Hemagglutinin
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-07-01 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 203.106, 83.279, 178.234 |
格子定数 [度] | 90.00, 106.67, 90.00 |
精密化法
残基 | 20.000 - 2.700 |
R因子 | 0.248 |
Rwork | 0.248 |
R-free | 0.26500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ru7 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 20.000 | 2.820 |
分解能 [Å] (高) | 2.700 | 2.700 |
Rmerge_l_obs | 0.084 | 0.324 |
独立反射数 | 73352 | |
<I/σ(I)> | 7.8 | 2 |
完全性 [%] | 90.5 | 68.4 |
冗長性 | 9.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 291 | Peg5K MME, TrisHCl, Sodium citrate, pH 6.8, VAPOR DIFFUSION, HANGING DROP, temperature 291K |