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1RKE

Human vinculin head (1-258) in complex with human vinculin tail (879-1066)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 5.0.2
Synchrotron siteALS
Beamline5.0.2
Detector technologyCCD
Wavelength(s)0.9797
Spacegroup nameP 21 21 2
Unit cell lengths86.603, 161.648, 36.040
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution15.000 - 2.350
Rwork0.206
R-free0.27800
Structure solution methodSIRAS
RMSD bond length0.008
RMSD bond angle0.979
Data reduction softwared*TREK
Data scaling softwared*TREK
Phasing softwareSHARP
Refinement softwareBUSTER-TNT
Data quality characteristics
 Overall
Low resolution limit [Å]99.800
High resolution limit [Å]2.350
Number of reflections21798
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion

*

829315% PEG 3350; 50 mM NaCl; 100 mM Tris (pH 8); 10 mM DTT, pH 8.0, temperature 293K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirPEG335015 (%)
21reservoir50 (mM)
31reservoirTris100 (mM)pH8
41reservoirdithiothreitol10 (mM)

217705

數據於2024-03-27公開中

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