Loading
PDBj
メニューPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1RK2

E. COLI RIBOKINASE COMPLEXED WITH RIBOSE AND ADP, SOLVED IN SPACE GROUP P212121

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsEMBL/DESY, HAMBURG BEAMLINE X11
Synchrotron siteEMBL/DESY, HAMBURG
BeamlineX11
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date1998-05
DetectorMARRESEARCH
Spacegroup nameP 21 21 21
格子定数 [Å]55.201, 62.492, 337.800
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基13.000 - 2.250
Rwork0.228
R-free0.26500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1RKD: RESIDUES 4-9 44-93 123-241 AND 254-309
結合長の平均二乗偏差(RMSD) [Å]0.007
結合角の平均二乗偏差(RMSD) [度]1.440

*

Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareCNS (0.5)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)13.0002.290
分解能 [Å] (高)2.2502.250
Rmerge_l_obs0.0720.291
Total number of observations188129

*

独立反射数55979
<I/σ(I)>173.9
完全性 [%]99.198.8
冗長性44
結晶化条件
結晶ID方法pH温度溶液条件
1Vapor diffusion, hanging drop

*

4.820

*

CRYSTALS WERE GROWN IN THE PRESENCE OF 5 MM RIBOSE, 10 MM ADP, 0.05 MM ALF4 AND 15 MM NAF USING 8.8-15% PEG 4000, 0.25 M MGCL2 AND 20% MPD IN 0.1 M TRIS- HCL BUFFERED TO PH 4.8.
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11dropribokinase3-3.5 (mg/ml)
21reservoirribose5 (mM)
31reservoirADP10 (mM)
41reservoirAIF30.05 (mM)
51reservoir15 (mM)
61reservoirsodium acetate0.1 (M)
71reservoir0.25 (M)
81reservoirMPD20 (%(v/v))
91reservoirPEG40008.8-15 (%(w/v))

217705

件を2024-03-27に公開中

PDB statisticsPDBj update infoContact PDBjnumon