1RGQ

M9A HCV Protease complex with pentapeptide keto-amide inhibitor

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	100
Detector technology	CCD
Collection date	1999-01-08
Detector	MARRESEARCH
Wavelength(s)	1.54
Spacegroup name	H 3 2
格子定数 [Å]	226.385, 226.385, 76.864
格子定数 [度]	90.00, 90.00, 120.00

精密化法

残基	34.120 - 2.900
Rwork	0.279
R-free	0.31200
Structure solution method	MOLECULAR REPLACEMENT
結合長の平均二乗偏差(RMSD) [Å]	0.013
結合角の平均二乗偏差(RMSD) [度]	1.700
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	CNX
Refinement software	CNX

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	34.120	3.000
分解能 [Å] (高)	2.900	2.900
独立反射数	16212
完全性 [%]	96.7	100

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	6.5	298	0.2M N/KPO4, 2.0M NaCl, 10mM MES, 15% glycerol, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K