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1RF3

Structurally Distinct Recognition Motifs in Lymphotoxin-B Receptor and CD40 for TRAF-mediated Signaling

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL9-1
Synchrotron siteSSRL
BeamlineBL9-1
Temperature [K]98
Detector technologyIMAGE PLATE
Collection date2001-10-18
DetectorMARRESEARCH
Wavelength(s)1.000
Spacegroup nameP 3 2 1
Unit cell lengths83.700, 83.700, 79.100
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution8.000 - 3.500
Rwork0.266
R-free0.31500
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)1l0a
RMSD bond length0.009
RMSD bond angle1.520
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0003.630
High resolution limit [Å]3.5003.500
Number of reflections3177
<I/σ(I)>88
Completeness [%]95.495
Redundancy4.43
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.529415% PEG4000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 294K

217705

건을2024-03-27부터공개중

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