Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1R78

CDK2 complex with a 4-alkynyl oxindole inhibitor

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X8C
Synchrotron siteNSLS
BeamlineX8C
Temperature [K]110
Detector technologyCCD
Collection date1999-10-06
DetectorADSC QUANTUM 4
Wavelength(s)0.979
Spacegroup nameP 21 21 21
Unit cell lengths53.880, 71.962, 72.779
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution51.300 - 2.000
R-factor0.21999
Rwork0.218
R-free0.27300

*

Structure solution methodrigid body refinement
RMSD bond length0.010
RMSD bond angle1.243
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwareREFMAC (5.1.24)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.070
High resolution limit [Å]2.0002.000
Rmerge0.0360.050
Number of reflections18512
Completeness [%]93.669.1
Redundancy3.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION9277pH 9, VAPOR DIFFUSION, temperature 277K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein12 (mg/ml)
21reservoirPEG335010 (%)
31reservoirCHES0.1 (M)pH9.
41reservoirbeta-mercaptoethanol2.5 (%)

217705

数据于2024-03-27公开中

PDB statisticsPDBj update infoContact PDBjnumon