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1PZD

Structural Identification of a conserved appendage domain in the carboxyl-terminus of the COPI gamma-subunit.

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsCHESS BEAMLINE A1
Synchrotron siteCHESS
BeamlineA1
Wavelength(s)0.92
Spacegroup nameP 21 21 21
Unit cell lengths49.570, 89.560, 98.600
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution43.190 - 2.310
R-factor0.199
Rwork0.199
R-free0.23600
Structure solution methodMAD
RMSD bond length0.006
RMSD bond angle25.100

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Data reduction softwareMOSFLM
Data scaling softwareSCALEPACK
Phasing softwareSnB
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]44.0002.440
High resolution limit [Å]2.3002.300
Number of reflections19621
<I/σ(I)>6.3
Completeness [%]89.787.5
Redundancy4.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.5

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20

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100mM sodium citrate and 1.5-1.7M lithium chloride, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 18K
1VAPOR DIFFUSION, SITTING DROP7.5

*

20

*

100mM sodium citrate and 1.5-1.7M lithium chloride, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 18K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein20 (mg/ml)
21dropTris20 (mM)pH7.5
31reservoir1.4-1.7 (M)
41reservoirsodium citrate100 (mM)pH6.0

217705

건을2024-03-27부터공개중

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