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1PRY

Structure Determination of Fibrillarin Homologue From Hyperthermophilic Archaeon Pyrococcus furiosus (Pfu-65527)

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 17-ID
Synchrotron siteAPS
Beamline17-ID
Temperature [K]100
Detector technologyCCD
Collection date2001-10-16
DetectorMARRESEARCH
Wavelength(s)1.74
Spacegroup nameP 21 21 21
格子定数 [Å]43.967, 62.082, 103.363
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基40.060

*

- 1.970
R因子0.228

*

Rwork0.204
R-free0.27200

*

Structure solution methodSingle Anomalous Scattering
結合長の平均二乗偏差(RMSD) [Å]0.006

*

結合角の平均二乗偏差(RMSD) [度]1.300

*

Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Refinement softwareCNS (1.1)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)40.4602.050
分解能 [Å] (高)1.9701.970
Rmerge_l_obs0.052

*

独立反射数18879
<I/σ(I)>19.4
完全性 [%]82.3

*

33.9
結晶化条件
結晶ID方法pH温度溶液条件
1Batch method

*

8.518

*

PEG 6000, ammonium phosphate, pH 8.5, Microbatch, temperature 291K
1Batch method

*

8.518

*

PEG 6000, ammonium phosphate, pH 8.5, Microbatch, temperature 291K
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
111PEG800010 (%)
211calcium acetate200 (mM)
311imidazole100 (mM)pH8.0
411PEG600012 (%)
511di-ammonium hydrogen phosphate100 (mM)
611Tris-HCl100 (mM)pH8.5

217705

件を2024-03-27に公開中

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