1OCO
BOVINE HEART CYTOCHROME C OXIDASE IN CARBON MONOXIDE-BOUND STATE
Experimental procedure
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 283 |
Detector technology | IMAGE PLATE |
Collection date | 1996-07-21 |
Detector | FUJI |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 189.100, 210.500, 178.600 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 7.000 - 2.800 |
R因子 | 0.213 |
Rwork | 0.213 |
R-free | 0.25600 |
Structure solution method | MULTIPLE ISOMORPHOUS REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.014 |
結合角の平均二乗偏差(RMSD) [度] | 26.149 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.84) |
Refinement software | X-PLOR (3.84) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 100.000 | 2.900 |
分解能 [Å] (高) | 2.800 | 2.800 |
Rmerge_l_obs | 0.062 * | 0.320 * |
Total number of observations | 1656746 * | |
独立反射数 | 173384 | 14954 * |
<I/σ(I)> | 14.7 | 3.5 |
完全性 [%] | 97.5 | 85 |
冗長性 | 9.5 | 3.3 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | unknown * | 6.8 | pH 6.8 |