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1NU9

Staphylocoagulase-Prethrombin-2 complex

Experimental procedure
実験手法MAD
Source typeSYNCHROTRON
Source detailsMPG/DESY, HAMBURG BEAMLINE BW6
Synchrotron siteMPG/DESY, HAMBURG
BeamlineBW6
Temperature [K]100
Detector technologyCCD
Collection date2002-08-01
DetectorMARRESEARCH
Wavelength(s)1.0092, 1.0000, 0.9500
Spacegroup nameC 1 2 1
格子定数 [Å]181.160, 102.340, 135.540
格子定数 [度]90.00, 129.91, 90.00
精密化法
残基19.980 - 2.200
R因子0.217
Rwork0.210
R-free0.25300
Structure solution methodMAD
結合長の平均二乗偏差(RMSD) [Å]0.011
結合角の平均二乗偏差(RMSD) [度]1.600
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS (1.1)
Quality characteristics
 OverallOuter shell
分解能 [Å] (高)2.100

*

Rmerge_l_obs0.039

*

0.260

*

独立反射数110836

*

完全性 [%]91.1

*

83.4

*

結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, HANGING DROP7.5291100mM imidazole, 200mM sodium formate, 12%(w/v) PEG 4000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11reservoirimidazole100 (%(v/v))pH7.5
21reservoirsodium formate200 (mM)
31reservoirPEG400012 (%(w/v))

217705

件を2024-03-27に公開中

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