1MZ4
Crystal Structure of Cytochrome c550 from Thermosynechococcus elongatus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X8C |
Synchrotron site | NSLS |
Beamline | X8C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-06-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.100 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 69.641, 69.641, 92.849 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.580 - 1.800 |
R-factor | 0.182 |
Rwork | 0.182 |
R-free | 0.20200 |
Structure solution method | two wavelength anomalous dispersion |
RMSD bond length | 0.006 |
RMSD bond angle | 1.800 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 25953 | |
<I/σ(I)> | 25.2 | 4.6 |
Completeness [%] | 98.2 | 96.7 |
Redundancy | 7.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | 2 M dihydrogen phosphate, MES, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |