1MHN

High resolution crystal structure of the SMN Tudor domain

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID29
Synchrotron site	ESRF
Beamline	ID29
Temperature [K]	100
Detector technology	CCD
Collection date	2001-12-01
Detector	ADSC QUANTUM 4
Wavelength(s)	0.934
Spacegroup name	P 65
格子定数 [Å]	27.652, 27.652, 110.299
格子定数 [度]	90.00, 90.00, 120.00

精密化法

残基	23.947 - 1.800
R因子	0.1466
Rwork	0.144
R-free	0.18710
Structure solution method	MOLECULAR REPLACEMENT
結合長の平均二乗偏差(RMSD) [Å]	0.014 *
結合角の平均二乗偏差(RMSD) [度]	1.341 *
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	CNS
Refinement software	CNS

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	23.950	1.900
分解能 [Å] (高)	1.800	1.800
独立反射数	4499
完全性 [%]	100.0	100
冗長性	11.4

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	4.5	285	Sprangers, R., (2003) Acta Crystallogr., D59, 366. *