1KZZ

DOWNSTREAM REGULATOR TANK BINDS TO THE CD40 RECOGNITION SITE ON TRAF3

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.1
Synchrotron site	ALS
Beamline	5.0.1
Temperature [K]	110
Detector technology	CCD
Collection date	2000-09-06
Detector	ADSC QUANTUM 4
Wavelength(s)	0.9200
Spacegroup name	P 3 2 1
格子定数 [Å]	82.500, 82.500, 77.900
格子定数 [度]	90.00, 90.00, 120.00

精密化法

残基	50.000 - 3.500
R因子	0.225 *
Rwork	0.225
R-free	0.30700
Structure solution method	MOLECULAR REPLACEMENT
結合長の平均二乗偏差(RMSD) [Å]	0.010
結合角の平均二乗偏差(RMSD) [度]	1.540
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	50.000	3.610
分解能 [Å] (高)	3.500	3.500
Rmerge_l_obs	0.079 *
Total number of observations	22731 *
独立反射数	4458 *
完全性 [%]	99.9 *	99.9
冗長性	5.1

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	6.7	298	unpublished data *