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1JF2

Crystal Structure of W92F obelin mutant from Obelia longissima at 1.72 Angstrom resolution

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2001-04-08
DetectorRIGAKU RAXIS IV
Wavelength(s)1.5418
Spacegroup nameP 41 21 2
格子定数 [Å]53.449, 53.449, 144.485
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基26.280 - 1.720
R因子0.232
Rwork0.232
R-free0.27400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1el4
結合長の平均二乗偏差(RMSD) [Å]0.005
結合角の平均二乗偏差(RMSD) [度]1.100
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)30.0001.760
分解能 [Å] (高)1.7001.700
Rmerge_l_obs0.037

*

0.080

*

独立反射数21633
<I/σ(I)>18.08
完全性 [%]99.9

*

87.7
冗長性5.8

*

10.2
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, HANGING DROP64

*

Deng, L., (2001) FEBS Lett., 506, 281.

*

文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11dropprotein8-10 (mg/ml)
21reservoirPEG800018 (%)
31reservoirpotassium phosphate50 (mM)
41drophexamine cobalt chloride

217705

件を2024-03-27に公開中

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