1J48
Crystal Structure of Apo-C1027
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE |
| Synchrotron site | SRS |
| Temperature [K] | 115 |
| Detector technology | CCD |
| Collection date | 2001-02-05 |
| Detector | MARRESEARCH |
| Spacegroup name | P 31 |
| Unit cell lengths | 55.150, 55.150, 55.870 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 500.000 - 1.800 |
| Rwork | 0.185 |
| R-free | 0.23700 |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.730 |
| Data reduction software | DENZO (2000) |
| Data scaling software | SCALEPACK (2000) |
| Refinement software | CNS (1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.730 |
| High resolution limit [Å] | 1.600 | 1.700 |
| Rmerge | 0.076 | 0.650 |
| Number of reflections | 41467 | |
| <I/σ(I)> | 3 | |
| Completeness [%] | 91.3 | 87.4 |
| Redundancy | 2.3 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | HANGING DROP/VAPOR DIFFUSION | 6.5 | 291 | Ammonium sulfate, Cacodylic acid, pH 6.5, HANGING DROP/VAPOR DIFFUSION, temperature 291.0K |
