1J48

Crystal Structure of Apo-C1027

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SRS BEAMLINE
Synchrotron site	SRS
Temperature [K]	115
Detector technology	CCD
Collection date	2001-02-05
Detector	MARRESEARCH
Spacegroup name	P 31
格子定数 [Å]	55.150, 55.150, 55.870
格子定数 [度]	90.00, 90.00, 120.00

精密化法

残基	500.000 - 1.800
Rwork	0.185
R-free	0.23700
結合長の平均二乗偏差(RMSD) [Å]	0.014
結合角の平均二乗偏差(RMSD) [度]	1.730
Data reduction software	DENZO (2000)
Data scaling software	SCALEPACK (2000)
Refinement software	CNS (1.0)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	50.000	1.730
分解能 [Å] (高)	1.600	1.700
Rmerge_l_obs	0.076	0.650
独立反射数	41467
<I/σ(I)>	3
完全性 [%]	91.3	87.4
冗長性	2.3	2

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	HANGING DROP/VAPOR DIFFUSION	6.5	291	Ammonium sulfate, Cacodylic acid, pH 6.5, HANGING DROP/VAPOR DIFFUSION, temperature 291.0K