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1HG4

Ultraspiracle ligand binding domain from Drosophila melanogaster

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSRS BEAMLINE PX9.6
Synchrotron siteSRS
BeamlinePX9.6
Temperature [K]100
Detector technologyCCD
DetectorADSC CCD
Spacegroup nameP 1
Unit cell lengths37.980, 86.190, 137.000
Unit cell angles85.57, 85.94, 83.09
Refinement procedure
Resolution34.000 - 2.400
R-factor0.248
Rwork0.248
R-free0.28400
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ere
RMSD bond length0.008
RMSD bond angle1.200
Data reduction softwareMOSFLM
Phasing softwareCNS (1.0)
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]34.000
High resolution limit [Å]2.2002.400

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Rmerge0.1260.305

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Total number of observations175324

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Number of reflections60384
<I/σ(I)>4.4
Completeness [%]90.0
Redundancy2.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion

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4.6

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18

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used streak-seeding

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Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein10 (mg/ml)
21reservoirammonium sulfate130 (mM)
31reservoirsodium acetate160 (mM)
41reservoirPEG200025 (%)

217705

数据于2024-03-27公开中

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