1FUO
FUMARASE C WITH BOUND CITRATE
Experimental procedure
Temperature [K] | 294 |
Detector technology | AREA DETECTOR |
Collection date | 1995 |
Detector | SIEMENS-NICOLET X100 |
Spacegroup name | C 2 2 21 |
格子定数 [Å] | 104.000, 219.900, 86.700 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 8.000 - 1.980 |
R因子 | 0.165 |
Rwork | 0.165 |
R-free | 0.20600 |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 21.050 * |
Data reduction software | XENGEN |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Quality characteristics
Overall | |
分解能 [Å] (高) | 1.980 * |
Rmerge_l_obs | 0.062 * |
独立反射数 | 69760 * |
完全性 [%] | 93.5 * |
冗長性 | 4.45 * |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | Vapor diffusion, hanging drop * | 6 * |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | reservoir | citrate | 300 (mM) | |
2 | 1 | reservoir | PEG4000 | 14 (%) |