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1EHW

HUMAN NUCLEOSIDE DIPHOSPHATE KINASE 4

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsLURE BEAMLINE DW32
Synchrotron siteLURE
BeamlineDW32
Temperature [K]277
Detector technologyIMAGE PLATE
DetectorMARRESEARCH
Spacegroup nameP 21 3
Unit cell lengths112.960, 112.960, 112.960
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000 - 2.400
R-factor0.184
Rwork0.184
R-free0.22900
RMSD bond length0.010
RMSD bond angle1.500
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareCNS (0.5)
Data quality characteristics
 Overall
Low resolution limit [Å]30.000
High resolution limit [Å]2.400
Rmerge0.105

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Total number of observations115939

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Number of reflections19054
Completeness [%]94.3

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Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.5291lithium sulfate, sodium chloride, HEPES, EDTA, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11drop150 (mM)
21dropEDTA5 (mM)
31dropHEPES100 (mM)
41drop0.7 (M)
51reservoir150 (mM)
61reservoirEDTA5 (mM)
71reservoirHEPES100 (mM)
81reservoir1.4 (M)
91dropprotein4 (mg/ml)

217705

数据于2024-03-27公开中

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