1DTN
MANDELATE RACEMASE MUTANT D270N CO-CRYSTALLIZED WITH (S)-ATROLACTATE
Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1992-06-03 |
Detector | SIEMENS |
Spacegroup name | I 4 2 2 |
格子定数 [Å] | 125.500, 125.500, 107.300 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 20.000 - 2.100 |
R因子 | 0.171 * |
Rwork | 0.171 |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 2.200 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | X-PLOR |
Refinement software | TNT |
Quality characteristics
Overall | |
Rmerge_l_obs | 0.130 |
独立反射数 | 24924 |
完全性 [%] | 85.3 |
冗長性 | 2.7 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | Vapor diffusion, hanging drop * | 7.5 * |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | drop | Tris | 50 (mM) | |
2 | 1 | drop | 10 (mM) | ||
3 | 1 | drop | (S)-atrolactate | 50 (mM) | |
4 | 1 | drop | E317Q | 13 (mg/ml) | |
5 | 1 | drop | atrolactate | 5 (mM) | |
6 | 1 | reservoir | 30 (%) | ||
7 | 1 | reservoir | acetone | 3 (%(v/v)) |