1DJ7
CRYSTAL STRUCTURE OF FERREDOXIN THIOREDOXIN REDUCTASE
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, Hamburg |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | AREA DETECTOR |
Collection date | 1998-07-18 |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
格子定数 [Å] | 45.296, 45.296, 172.147 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 10.000 - 1.600 |
R因子 | 0.264 |
Rwork | 0.238 |
R-free | 0.27800 |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.800 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | REFMAC |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 15.000 | 1.600 |
分解能 [Å] (高) | 1.500 | 1.500 |
Rmerge_l_obs | 0.049 | 0.196 |
独立反射数 | 26709 | |
<I/σ(I)> | 10.93 | |
完全性 [%] | 88.8 | |
冗長性 | 3 | 2.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 * | 297 | drop consists of equal volume of protein and reservoir solutions * |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | drop | protein | 17 (mg/ml) | |
2 | 1 | drop | triethanolamine-HCl | 20 (mM) | |
3 | 1 | reservoir | ammonium sulfate | 2.0 (M) | |
4 | 1 | reservoir | ammonium sulfate | 2.0 (M) | |
5 | 1 | reservoir | 0.1 (M) | ||
6 | 1 | reservoir | 100 (mM) |